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  • Internal Standard and Deuterated Solvent Selection: A Crucial Step in PFAS-based Fluorine-19 (¹⁹F) NMR Research

    Purpose: This work is vital because it provides researchers with a framework and rationale for selecting the best internal standard and deuterated solvent for their nuclear magnetic resonance (NMR) analysis of per- and polyfluoroalkyl substances (PFAS)-based compounds. Selecting the best internal standard and deuterated solvent will help to ensure that their results are accurate, precise, and sensitive. The internal standard that is chosen can significantly affect the accuracy, precision, sensitivity, and quantification of NMR measurements. Therefore, it is essential to carefully select an internal standard and a matching deuterated solvent that are well-suited for analyzing PFAS compounds.
  • Optimization of LC-MS/MS Parameters for Analysis of Per- and Polyfluoroalkyl Substances (PFAS)

    Purpose: Integrate US Environmental Protection Agency (USEPA) Method 537 on current instrumentation to provide per- and polyfluoroalkyl substances (PFAS) analytical capabilities for the US Army Engineer Research and Development Center (ERDC), US Army Corps of Engineers (USACE) and the Department of Defense (DoD).